6-broMo-2,3-dihydro-1H-inden-5-ol
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6-broMo-2,3-dihydro-1H-inden-5-ol
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CAS No:
32337-85-2
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Formula:
C9H9BrO
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Chemical Name:
6-broMo-2,3-dihydro-1H-inden-5-ol
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Synonyms:
6-Bromo-2,3-dihydro-1H-inden-5-ol;6-BROMOINDAN-5-OL;SCHEMBL650257;DTXSID40576234;ZINC34616592;AKOS023784835;CS-W006555;DS-9583;AK167878
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CAS No:
6-broMo-2,3-dihydro-1H-inden-5-ol Use and Manufacturing
The 5 - [...] (268 g, 2 µM) dissolved in 400 ml N, N - dimethyl formamide (DMF) in, lowering the temperature to 0 °C, batch slowly adding N - bromo succinimide (NBS) (2.1 µM), maintaining the reaction temperature at 2 °C the left and the right reaction 6 h, TLC monitoring after the reaction, the reaction liquid is poured into the 3 L in water, the extraction of ethyl acetate (500 ml × 4), organic uses 1 N hydrochloric acid solution of extraction (500 ml × 2), then the saturated salt water for extraction (500 ml × 2), anhydrous sodium sulfate drying, concentrated under reduced pressure to obtain brown oily matter. The oil thing and molecular distillation (conditions: 70 °C, 100 pa) is light component is 4 - bromo - 2, 3 - dihydronaphth - 1H - indenyl -5 - alcohol (103.8 g).
Computed Properties
Molecular Weight:213.07
XLogP3:3.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Exact Mass:211.98368
Monoisotopic Mass:211.98368
Topological Polar Surface Area:20.2
Heavy Atom Count:11
Complexity:149
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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Business licensed Certified factoryManufactory Supplier of 4-(Pentafluorothio)aniline,Pentafluoro,Pentafluorothio,Pentafluorosulfur,[4-(bromomethyl)phenyl]-pentafluoro-lambda6-sulfane,[4-(pentafluoro-sulfanyl)phenyl]acetic acidInquiryCAS No.: 32337-85-2Grade: Industrial GradeContent: 95%
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6-broMo-2,3-dihydro-1H-inden-5-ol
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